Mettler Toledo GA42 Instructions d'exploitation

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Operating Instructions
METTLER TOLEDO
DE40, DE50 and DE51 Density Meters
V2.00
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Résumé du contenu

Page 1 - METTLER TOLEDO

Operating InstructionsMETTLER TOLEDODE40, DE50 and DE51 Density MetersV2.00

Page 2

10 METTLER TOLEDO DE40/50/51 Density MeterDensityThe here described period of oscillation T is used to calculate the tube factor and from thatthe den

Page 3 - Contents Page

METTLER TOLEDO DE40/50/51 Density Meter 113.3 Construction of the measuring cell and temperature controlFor correct density measurements a very accur

Page 4 - Contents

12 METTLER TOLEDO DE40/50/51 Density Meter4. The instrumentFront viewThe instrument6. Memory card slot3. Cell window2. Measuring cell1. DesiccatorFor

Page 5 - DE40/50/51 Density Meter 5

METTLER TOLEDO DE40/50/51 Density Meter 13The instrumentRear view17. Pump in connector(only with ASU-DE)13. Measuring cell out14. Measuring cell in15

Page 6 - 1. Introduction

14 METTLER TOLEDO DE40/50/51 Density Meter8DEF9GHI4JKL5MNO6PQR1STU2VWX3YZ.0BLK-Func.SetupDisplayReport MethodPrintEnterResetCheckClearSampleEsc.BSCal

Page 7 - 2. Safety measures

METTLER TOLEDO DE40/50/51 Density Meter 15Method: Key to select the method (0 to 9). The selection is done either bypressing the "Up" and &

Page 8 - 3. The density

16 METTLER TOLEDO DE40/50/51 Density MeterPump For ASU-DE sampling pump. Starts and stops the pump.Clear: Key to erase the whole entry (2 x to clear

Page 9

METTLER TOLEDO DE40/50/51 Density Meter 174.3 DisplayThe DE40, DE50 and DE51 density meters have a seven line LCD display with 40 charactersper line.

Page 10 - End value

18 METTLER TOLEDO DE40/50/51 Density Meter5. Getting startedBefore connecting the power cord after unpacking the instrument loosen or remove the thre

Page 11

METTLER TOLEDO DE40/50/51 Density Meter 195.1.2 Date and time (Setup 1)- Press the <SETUP> key.Select "1.Date&Time". Confirm with

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20 METTLER TOLEDO DE40/50/51 Density MeterThe earlier used term calibration should not be used anymore for this purpose as soon asinstrument settings

Page 14

METTLER TOLEDO DE40/50/51 Density Meter 215.2.3 Performing the air adjustmentWhether you have a sampling pump ASU-DE or not, the following steps will

Page 15

22 METTLER TOLEDO DE40/50/51 Density Meter- Leave the syringe in the sample inlet .- Press <ENTER>.While adjusting to the water valuethe displa

Page 16

METTLER TOLEDO DE40/50/51 Density Meter 235.3 Perform a measurementPerform for example two measurements with your standard sample.5.3.1 Set the param

Page 17 - The instrument

24 METTLER TOLEDO DE40/50/51 Density MeterGetting started5.3.3 Sampling with ASU-DE- Dip the sampling tube into the beaker containing your sample.- P

Page 18 - 5. Getting started

METTLER TOLEDO DE40/50/51 Density Meter 250.TestMeth ORANGE 02-01Temp.(°C) Density(g/cm3)Set 20.00Cell 20.00

Page 19 - Getting started

26 METTLER TOLEDO DE40/50/51 Density Meter6. Sample (Number and ID) and Sample FileHere you can define your sample identifications like sample number

Page 20 - Purge Checking

METTLER TOLEDO DE40/50/51 Density Meter 27Method:Here you can select if you want to perform all measurements with one method only (currentmethod) or

Page 21 - DE40/50/51 Density Meter 21

28 METTLER TOLEDO DE40/50/51 Density Meter6.2 Viscosity correctionFor viscosity corrected measurements the instrument has to be adjusted with the vis

Page 22

METTLER TOLEDO DE40/50/51 Density Meter 297. Report (password protected)In the <REPORT> menu you can choose the format of your printout accordi

Page 23 - DE40/50/51 Density Meter 23

METTLER TOLEDO DE40/50/51 Density Meter 3Contents Page1. Introduction ...

Page 24

30 METTLER TOLEDO DE40/50/51 Density Meter8. Measuring parameter (password protected)This section describes how to set the measuring parameters for t

Page 25 - Set Rinse-1

METTLER TOLEDO DE40/50/51 Density Meter 318.2 Measuring temperatureThis option is used to set the measuring temperature.Enter your measuring temperat

Page 26 - Sample and sample file

32 METTLER TOLEDO DE40/50/51 Density Meter8.4 Limit timeThis option is used to set the limit time. When this time limit is reached, the measurement i

Page 27 - DE40/50/51 Density Meter 27

METTLER TOLEDO DE40/50/51 Density Meter 33Measuring parametersO.S.Rate: The instrument will detect how much time it needs from starting the pumpuntil

Page 28 - Measuring

34 METTLER TOLEDO DE40/50/51 Density MeterMeasuring parametersMethod 0 < Meas.Parameter > VACell Test :Off OnCalib. :<Other STD>STD-

Page 29 - DE40/50/51 Density Meter 29

METTLER TOLEDO DE40/50/51 Density Meter 35Note: The Cell Test is not available if you select "Other STD". Only very accurate densitystandar

Page 30 - Measuring parameters

36 METTLER TOLEDO DE40/50/51 Density Meter9. Calculation parameters (password protected)This section describes how to select the type of results (den

Page 31 - DE40/50/51 Density Meter 31

METTLER TOLEDO DE40/50/51 Density Meter 37ConcentrationSelect "Conc." with the → key.Confirm with <ENTER>.You will select this option

Page 32

38 METTLER TOLEDO DE40/50/51 Density MeterSelect "Coefficient" with the → key.Confirm with <ENTER>.Select "x <- d" with

Page 33 - DE40/50/51 Density Meter 33

METTLER TOLEDO DE40/50/51 Density Meter 39Concentration table for sulfuric acid (from "Handbook of Chemistry and Physics").Note: see our In

Page 34

4 METTLER TOLEDO DE40/50/51 Density MeterContentsPage10. Functions (password protected) ...

Page 35 - DE40/50/51 Density Meter 35

40 METTLER TOLEDO DE40/50/51 Density MeterThe results of the calculation areshown and can be printed.Constants usedThe A, B and C values are the coef

Page 36 - Calculation parameters

METTLER TOLEDO DE40/50/51 Density Meter 419.3 Temperature compensationThis section describes how to set the temperature compensation. It allows to me

Page 37 - DE40/50/51 Density Meter 37

42 METTLER TOLEDO DE40/50/51 Density MeterThere are two ways to program a temperature compensation function, either by entering thisfunction directly

Page 38 - Result

METTLER TOLEDO DE40/50/51 Density Meter 4310. Functions (password protected)10.1 Data File (Function 0)This function allows to view and process the m

Page 39 - DE40/50/51 Density Meter 39

44 METTLER TOLEDO DE40/50/51 Density MeterAfter selecting <Statis.> and con-firmation with <ENTER>, you canselect the filter to process o

Page 40

METTLER TOLEDO DE40/50/51 Density Meter 45FunctionsPress the <CALC.PARA> key.Select "1.Result" and confirm with<ENTER>Select Br

Page 41 - DE40/50/51 Density Meter 41

46 METTLER TOLEDO DE40/50/51 Density MeterNow you can resume the statistics calculation again and then print the results without themarked measuremen

Page 42

METTLER TOLEDO DE40/50/51 Density Meter 47FunctionsSelecting Calib. "On" means that inthe starting position there has to bea vial with dei

Page 43 - Functions

48 METTLER TOLEDO DE40/50/51 Density MeterFunctions10.6.1 Daily CheckThis check is used mainly to control the working condition of the instrument. Is

Page 44

METTLER TOLEDO DE40/50/51 Density Meter 49We recommend to use our certified density standards for a periodic instrument check:ME-51338002 Water 0.99.

Page 45 - Recalculation

METTLER TOLEDO DE40/50/51 Density Meter 5Contents13. Application Memory Cards: BRIX, ALCOHOL, API, VISCOSITY CORREC-TION, USER TABLES ...

Page 46

50 METTLER TOLEDO DE40/50/51 Density MeterFunctionsSelect Show Check List Execute todisplay the list of the last 10 checksperformedThe whole list can

Page 47 - DE40/50/51 Density Meter 47

METTLER TOLEDO DE40/50/51 Density Meter 51FunctionsIf "On" is selected, the instrument will give one of the following messages when it is t

Page 48

52 METTLER TOLEDO DE40/50/51 Density MeterWhen you have chosen "On", youcan define the time interval betweentwo measurements. Confirm with&

Page 49 - DE40/50/51 Density Meter 49

METTLER TOLEDO DE40/50/51 Density Meter 53 < Memory Clear >0.Measured Data 4.Method Parameter1.Sample File 5.All Parameter2.P

Page 50

54 METTLER TOLEDO DE40/50/51 Density Meter11. Setup (password protected)11.1 Interface (Setup 0)This option is used to define the RS-232C serial inte

Page 51 - DE40/50/51 Density Meter 51

METTLER TOLEDO DE40/50/51 Density Meter 5511.1.2 Printer setupWe recommend to select the GA42 printer from METTLER TOLEDO. Make sure that the DIPswit

Page 52

56 METTLER TOLEDO DE40/50/51 Density MeterSetup11.3 Name (Setup 2)This option is used to enter the laboratory name (or company or operator).Press the

Page 53 - DE40/50/51 Density Meter 53

METTLER TOLEDO DE40/50/51 Density Meter 5711.5 LCD Contrast (Setup 4)This option is used to adjust the contrast of the LCD display in your instrument

Page 54

58 METTLER TOLEDO DE40/50/51 Density Meter11.7 Lock with password (Setup 6)Press the <SETUP> key.Select "6.Lock".Confirm with <ENT

Page 55 - DE40/50/51 Density Meter 55

METTLER TOLEDO DE40/50/51 Density Meter 59 < Setup >0.Interface 5.International1.Date & Time 6.Lock2.Name

Page 56

6 METTLER TOLEDO DE40/50/51 Density Meter1. IntroductionThe DE40 and DE50/DE51 Density Meters measure the density d of gases, liquids andsolutions us

Page 57 - DE40/50/51 Density Meter 57

60 METTLER TOLEDO DE40/50/51 Density Meter12. Memory Cards (DE40, DE50 and DE51)The following two sections describe the use of the memory cards. Ther

Page 58

METTLER TOLEDO DE40/50/51 Density Meter 6112.2 Save measured dataWith the Data Memory Card you can save data on the card or load data from the card.

Page 59 - °C (in equilibrium)

62 METTLER TOLEDO DE40/50/51 Density MeterWait until all data have been saved.Press <ENTER>.Your data are now saved on the memory card, you can

Page 60 - Data Memory Card

METTLER TOLEDO DE40/50/51 Density Meter 6312.4 Load measured dataThis may be used for example to recalculate some results you have already stored on

Page 61 - DE40/50/51 Density Meter 61

64 METTLER TOLEDO DE40/50/51 Density MeterYou can now display the loadeddata. Press the <FUNC> key.Select “0.Data File”. Confirm with<ENTER&

Page 62

METTLER TOLEDO DE40/50/51 Density Meter 65Wait until method has been saved.Press <ENTER>.12.6 Clear internal methodLet’s assume that you have s

Page 63 - DE40/50/51 Density Meter 63

66 METTLER TOLEDO DE40/50/51 Density Meter12.7 Load methodPress the <FUNC> key.Select “2.Method File”. Confirm with<ENTER>.First you have

Page 64

METTLER TOLEDO DE40/50/51 Density Meter 67Repeat the previous steps if youwant to load more methods, beingcareful not to overwrite an alreadydefined

Page 65 - DE40/50/51 Density Meter 65

68 METTLER TOLEDO DE40/50/51 Density MeterEnter the name under which youwant to store the sample file (max. 8characters).Press <ENTER> twice (c

Page 66

METTLER TOLEDO DE40/50/51 Density Meter 6912.10 Load sample filePress the <SAMPLE> key.Select “Load” with the → key.Confirm with <ENTER>.

Page 67 - DE40/50/51 Density Meter 67

METTLER TOLEDO DE40/50/51 Density Meter 7Safety measures2. Safety measuresMeasures for your safety– Ensure that you plug the power cable supplied int

Page 68

70 METTLER TOLEDO DE40/50/51 Density Meter13. Application Memory Cards: BRIX, ALCOHOL, API, VISCOSITYCORRECTION, USER TABLESThese Application Memory

Page 69 - DE40/50/51 Density Meter 69

METTLER TOLEDO DE40/50/51 Density Meter 71Wait until the installation has beendone.Press <ENTER>.The asterisk (*) on the left of theapplication

Page 70 - CORRECTION, USER TABLES

72 METTLER TOLEDO DE40/50/51 Density Meter13.2.1 Select a concentration table: ALCOHOL, BRIX, CONCENTRATIONSPress the <CALC.PARA> key.Select “1

Page 71 - Application Memory Card

METTLER TOLEDO DE40/50/51 Density Meter 7313.3 How to retrieve an application (Uninstall table)This section will show you how to retrieve an applicat

Page 72

74 METTLER TOLEDO DE40/50/51 Density MeterPress <ENTER>.Select “2.Exit” and confirm with<ENTER>.The table on the Memory Card is nolonger

Page 73 - DE40/50/51 Density Meter 73

METTLER TOLEDO DE40/50/51 Density Meter 75Special application cards14. Description of the special applications:BRIX, ALCOHOL, API, VISCOSITY CORRECTI

Page 74

76 METTLER TOLEDO DE40/50/51 Density Meter14.2.2 Temperature measured in °C, with a reference temperature at 20 °C:This option is activated by select

Page 75 - Special application cards

METTLER TOLEDO DE40/50/51 Density Meter 7714.5 Coke (Cola drinks)This Memory Card allows to measure BRIX and HFCS42 (also called SOLIDS) of all Colap

Page 76

78 METTLER TOLEDO DE40/50/51 Density Meter15. Automatic sampling pump ASU-DE (optional)This optional automatic sampling unit replaces the air pump t

Page 77

METTLER TOLEDO DE40/50/51 Density Meter 7915.2 Installation- Switch off the DE40/DE50/DE51 anddisconnect the power cable.- Place the unit backside d

Page 78 - Automatic sampling pump

8 METTLER TOLEDO DE40/50/51 Density MeterNote: The DE40/DE50/DE51 calculate the relative density: the density of water at 4 °C (dtt ) or at the measu

Page 79 - DE40/50/51 Density Meter 79

80 METTLER TOLEDO DE40/50/51 Density Meter- Install the ASU-DE in the place of the airpump.a) Slide in the ASU-DE down and to the left,adjusting its

Page 80

METTLER TOLEDO DE40/50/51 Density Meter 81Automatic sampling pumpWarning:If using samples and rinsing solutions whichcould create poisonous or corros

Page 81 - DE40/50/51 Density Meter 81

82 METTLER TOLEDO DE40/50/51 Density Meter16. Error Messages and Malfunctions16.1 Error MessagesError message Cause MeasureNozzle error The sampling

Page 82 - 16.2 Malfunction

METTLER TOLEDO DE40/50/51 Density Meter 83Malfunction Cause MeasureNothing displayed Contrast has been changed. Call METTLER TOLEDO servicefor help.N

Page 83

84 METTLER TOLEDO DE40/50/51 Density Meter17. Maintenance17.1 Changing internal batteryThe battery is used for data storage and has a service life of

Page 84 - 17. Maintenance

METTLER TOLEDO DE40/50/51 Density Meter 8518. Standard and optional equipment18.1 Standard equipmentOrder No.Operating instructions Englisch 51709838

Page 85 - DE40/50/51 Density Meter 85

86 METTLER TOLEDO DE40/50/51 Density MeterStandard and optional equipment18.2 Optional equipmentFuse T3.15A 51522100Plastic syringe 10mL (set of 100)

Page 86

METTLER TOLEDO DE40/50/51 Density Meter 87AD-510 Auto Drain Unit 51321807(requires ASU-DE)DCU-300B Auto Rinsing Unit 51321805(requires ASU-DE)CHG-260

Page 87 - DE40/50/51 Density Meter 87

88 METTLER TOLEDO DE40/50/51 Density MeterMemoCard DE40/50/51 (Short Instructions)Sample No, Sample ID(and number of samples ifSample file ON)Viscosi

Page 88

METTLER TOLEDO DE40/50/51 Density Meter 89Annex 1: Density table of dried airThe density of dried air at a specified temperature t and a atmospheric

Page 89 - Density tables

METTLER TOLEDO DE40/50/51 Density Meter 9DensityThe period of oscillation T is obtained from the equation:ρ = Density of sample in measurement tube [

Page 90

90 METTLER TOLEDO DE40/50/51 Density MeterAnnex 2: Density table of pure waterThe instrument has stored the density of water at 760 mmHg according to

Page 91 - Specifications

METTLER TOLEDO DE40/50/51 Density Meter 91SpecificationsSpecificationsType and model name Digital density meter DE40, DE50, DE51Measuring method Osci

Page 92

92 METTLER TOLEDO DE40/50/51 Density MeterFCC Rules and Radio Interference RegulationsThis equipment has been tested and found to comply with the lim

Page 94 - Thank you

To protect your METTLER TOLEDO product’s future:METTLER TOLEDO Service assures the quality, measuring accuracy andpreservation of value of all METTLER

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